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富氢水制备及保存方法的初步研究

秦秀军,安  全,张  伟,李建国,李炜宾,李幼忱,闻建华   

  1. ( 中国辐射防护研究院,山西  太原  030006 )
  • 收稿日期:2013-09-12 修回日期:2013-09-26 出版日期:2013-11-30 发布日期:2013-11-30
  • 通讯作者: 秦秀军,E-mail:qxj19982000 @163.com
  • 作者简介:秦秀军 (1979- ),男,山西省忻州市人,硕士,助理研究员,研究方向:辐射生物效应。Tel:0351-2203520,E-mail:qxj19982000 @163.com
  • 基金资助:

    中国辐射防护研究院青年科研基金项目 (2012年度)

Study of the preparation and the preservation method of the hydrogen-rich water

QIN Xiu-jun,AN Quan,ZHANG Wei,LI Jian-guo,LI Wei-bin,LI You-chen,WEN Jian-hua   

  1. (China Institute for Radiation Protection, Taiyuan 030006, Shanxi, China)
  • Received:2013-09-12 Revised:2013-09-26 Online:2013-11-30 Published:2013-11-30
  • Contact: QIN Xiu-jun,E-mail:qxj19982000 @163.com

摘要:

 目的: 建立富氢水的制备装置,制备富氢水,并对富氢水的保存方法进行初步研究。方法:采用增加压强的方法制备富氢水,研究不同通气压强 (0.1、0.2、0.3、0.4 MPa)、不同通气时间 (0.5、1、2、4、8 h)和不同抽真空时间 (0、5、10、30、60 min)对富氢水中氢气浓度的影响,同时观察温度、储存容器、放置时间、装量和滤膜抽滤对富氢水中氢气浓度变化的影响。结果:通气压强对氢气浓度无明显影响(P>0.05);通气时间和抽真空时间对氢气浓度有一定影响,维持通气4 h以上组较通气4 h以下组以及抽真空5 min以上组较未抽真空组氢气浓度均显著增加(P<0.05或P<0.01);氢气浓度会随着放置时间的延长而逐渐降低(P<0.05);氢气浓度变化与储存容器和保存温度无明显相关关系(P>0.05);氢气浓度变化与容器中富氢水是否装满有明显关系(P<0.05);滤膜抽滤会降低氢气浓度(P<0.05)。结论:在本研究条件下成功制备出一定浓度的富氢水,并对其保存方法有了初步了解。

关键词: 富氢水, 制备, 稳定性, 保存方法

Abstract:

 OBJECTIVE: Preliminary studies were performed on a device for preparing hydrogen-rich water,preparation of hydrogen-rich water,and hydrogen-rich water preservation method. METHODS:After preparation of hydrogen-rich water, the effect of the ventilation under different pressures (0.1,0.2,0.3,0.4 MPa),the different ventilation time (0.5,1,2,4,8 h) and the different vacuum time (0,5,10,30,60 min) on the hydrogen concentration of hydrogen-rich water were measured,and the impact of the temperature,storage containers,observing time,content and membrane filtration on the hydrogen concentration changes of hydrogen-rich water were also evaluated. RESULTS:The ventilation pressure had no significant effect on the hydrogen concentration(P>0.05).  Ventilation time and vacuum time showed a certain effect on hydrogen concentration when ventilating above 4 h or vacuum pumping more than 5 min,the hydrogen concentration increased significantly(P<0.05 or P<0.01),which was gradually decreased with the extension of storage time(P<0.05). The storage container and the temperature of preservation had no obviously effect on hydrogen concentration(P>0.05). The amount of water loaded had obvious effect on hydrogen concentration(P<0.05). Filtration reduced hydrogen concentration(P<0.05). CONCLUSION:We have successfully prepared hydrogen-rich water in certain concentration,and studied the preservation methods of hydrogen-rich water.

Key words: hydrogen-rich water, preparation, stability, preservation method