›› 2011, Vol. 23 ›› Issue (3): 199-201.doi: 10.3969/j.issn.1004-616x.2011.03.009

• 论著 • 上一篇    下一篇

海柳挥发性成分的分析

白雪婷1,陈一村1,陈伟洲2,雷华平3,石刚刚1,*   

  1. 1. 汕头大学医学院药理学研究室,广东 汕头 515041;2. 汕头大学海洋生物研究所,广东 汕头 515063;3. 中山大学生命科学学院,广东 广州 510275
  • 收稿日期:2011-03-03 修回日期:2011-04-12 出版日期:2011-05-30 发布日期:2011-05-30
  • 通讯作者: 石刚刚

Analysis of volatile components of black coral

BAI Xue-ting1,CHEN Yi-cun1,CHEN Wei-zhou2,LEI Hua-ping3,SHI Gang-gang1,*   

  1. 1.Department of Pharmacology, Shantou University Medical College, Shantou 515041; 2. Marine Biology Institute, Shantou University,Shantou 515063; 3. School of Life Sciences,Sun Yat-sen University, Guangzhou 510275, Guangdong, China
  • Received:2011-03-03 Revised:2011-04-12 Online:2011-05-30 Published:2011-05-30
  • Contact: SHI Gang-gang

摘要: 提取分离海柳的挥发性成分并鉴定。 方法:采用二氧化碳超临界萃取出海柳挥发性成分,再经气质联用分析,结合保留指数计算,鉴定其成分。 结果:通过气质联用分析,共鉴定出15种化学成分,包括磷酸三乙酯、丁羟甲苯、雪松醇、棕榈酸、角鲨烯、胆甾醇等。这些成分多具有生物活性。 结论:首次揭示海柳的挥发性成分,海柳所具有的功效可能与其含有的生物活性成分有关。

关键词: 海柳, 二氧化碳超临界萃取, 气质分析, 保留指数

Abstract: To investigate the volatile constituents of black coral (BC). METHODS:The volatile constituents of BC were extracted by supercritical fluid extraction with carbon dioxide (CO2-SFE),separated and identified by gas chromatography-mass spectrometry (GC-MS) combined with retention index . RESULTS:In total,15 components were reliably identified in BC and found to be biologically active. These included triethyl phosphate, butylated hydroxytoluene,cedrol,n-hexadecanoic acid,squalene and cholesterol. CONCLUSION: It is the first time that volatile constituents of BC were presented. The functions of BC are related to the active chemical compositions.

Key words: black corals, CO2-SFE, GC-MS, retention index